I'm trying to figure out what you really mean- what I'm interpreting is that a zone-valve on your hydronic (hot water) heating system has failed open, and you want to turn off the valve on a return line to stop a convective flow from bringing some heat into the zone even when the heating system's circulation pump isn't on. In most cases that would be safe, but more info would be useful. (To be sure replacing the defective valve before the heating season is advisable.)
BTW: Most people refer to the heat source of hydronic heating systems as a "boiler" rather than a "furnace" (as distinct from hot-air furnaces), even though the water isn't boiled to steam as in steam-heating systems. (The water actually DOES micro-boil at the heat exchanger plate surfaces, but the vast majority of the water is always liquid.)





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